Heidolph Synthesis 1 - Manual (Page 80)

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3. Coolant fitting, liquid- or solid-phase synthesis
3.1 Coolant connector, condensation zone
Use high-flexible tube (6 - 8 mm ID). Secure with tube clamps.
Do not impede shaking motion (orbit) of the reaction block by coolant
tubes.
3.2 Coolant fitting, conditioning zone for reactions below room
temperature.
Use high-flexible tube (6 - 8 mm ID). Insulate coolant tube when working below
freezing point. Secure with tube clamps.
Do not impede shaking motion (orbit) of the reaction block by coolant
tubes
4. Multiple-Evaporator
4.1 Reaction vessels
refer to Chapter 1.1 liquid-phase synthesis
4.2 Locate reaction vessels in heater block
refer to Chapter 1.2 liquid-phase synthesis
nipple, heater zone, OUT
nipple, coolant IN,
condensation zone
nipple, coolant return,
condensation zone
nipple, heater zone, IN