Heidolph Synthesis 1 - Manual (Page 57)

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4.1 Reaction vessels ................................................................................. 80
4.2 Locate reaction vessels in heater block .............................................. 80
4.3 Connect vacuum ................................................................................. 81
4.4 Set-up Synthesis 1 glassware kit for Multiple-Evaporator .................. 81
4.4.1 Set-up stand........................................................................................ 82
4.4.2 Install cooler ........................................................................................ 82
4.4.3 Connect vacuum and coolant.............................................................. 83
4.4.4 Install receiving flask ........................................................................... 83
4.5 Schematic, Multiple-Evaporator without vacuum control..................... 84
4.6 Schematic, Multi-Evaporator with vacuum control............................... 84
5. Electric wiring................................................................................................. 86
6. Install guard hood .......................................................................................... 86
6.1 Guard hood ......................................................................................... 86
6.2 Installation ........................................................................................... 87
7. Exchange reaction blocks .............................................................................. 87
OPERATION ............................................................................................................ 89
8.
General .......................................................................................................... 89
9. Controls, brief description .............................................................................. 89
9.1 Power switch ....................................................................................... 89
9.2 Start / Stop shaking action .................................................................. 89
9.3 Start / Stop heater ............................................................................... 90
9.4 Set / edit parameters........................................................................... 90
9.5 Set or display ...................................................................................... 90
9.6 Select value......................................................................................... 90
9.7 Set temperature gradient .................................................................... 90
9.8 Activate temperature gradients ........................................................... 90
9.9 Identic ................................................................................................. 90
10. Setting work in detail...................................................................................... 91
10.1 Set shaking frequency......................................................................... 91
10.2 Set temperature (4 heater zones with different temperatures) ............ 91
10.2.1 Setting................................................................................................. 91
10.2.2 Temperature setting, limiting values.................................................... 91
10.3
Set temperature (4 heater zones with same temperature) .................. 91
10.4 Set timer.............................................................................................. 91
10.5 Set temperature gradient .................................................................... 92
10.5.1 Set values ........................................................................................... 92
10.5.2 Delete values ...................................................................................... 93
10.5.3 Limiting temperatures.......................................................................... 93
10.6
Activate temperature gradient ............................................................. 93
10.7 Turn shaking action ON ...................................................................... 94
10.8 Turn heater ON ................................................................................... 94
11. External temperature sensor.......................................................................... 94
11.1 Temperatures below solvent's boil point ............................................. 95
11.2 Temperatures above solvent's boil point. ............................................ 95
11.3 In the use as multi evaporator ............................................................. 95
12. Setup (timer and temperature sensor) ........................................................... 96
13. Filter action, solid-phase synthesis ................................................................ 97
14. Use condensation zone ................................................................................. 98
15. Use heating zones with recirculating cooler (low temperature)...................... 98
16. Access to rear reaction vessels ..................................................................... 99
17. Interface RS 232 .......................................................................................... 100