Heidolph Synthesis 1 - Manual (Page 74)

74
E
2.1.7 Capacity of reaction vessels
Capacity of reaction vessels available for solid-phase syntheses are listed below:
item P/N total capacity
recommended
capacity
reaction vessel Solid 16 552-14230-00 42 ml 20 ml
reaction vessel Solid 20 552-12530-00 25 ml 12 ml
reaction vessel Solid 24 552-10830-00 12 ml 5 ml
2.2 Locate reaction vessels in heating- and condensation block
2.2.1 Install vessels
Seat reaction vessels in heating -/ condensation block as shown. Exert light pressure
to seat vessels. Elasticity of the shroud positively secures vessels. Vertical alignment:
clamping ring is in touch with heating block.
Handle hot reaction block with care; danger of burns. Use protective
gloves.
heating
block
clamping
ring