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Stirring – Metrohm 757 VA Computrace User Manual

Page 56

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3 General settings for exploratory and determination mode

757 VA Computrace – Software

46

2.

Purging
Optional purging of the sample solution during the

Initial purge

time

(details see Purging).

3.

Drop formation
Hg drop formation at the MME if

DME

,

SMDE

or

HMDE

is se-

lected (details see Electrodes, section 3.1).

4.

Conditioning cycles
Optional conditioning of solid state electrodes by applying
cyclic conditioning sweeps (details see Conditioning).

5.

Cleaning
Optional cleaning of solid state electrodes by applying a
cleaning potential during the

Cleaning time

(details see Pre-

treatment).

6.

Deposition
Optional electrochemical deposition for stripping voltammetry
during the

Deposition time

(details see Pretreatment).

7.

Equilibration time
Optional waiting time before starting the sweep. During the

Equilibration time

, the stirring is switched off and the

Start

po-

tential

is applied to the electrodes (details see Pretreatment).

8.

Voltage sweep
Start of the voltage sweep which depends on the selected
measurement mode (details see VA measurement modes,
section 3.2
).

9.

Stand-by potential
Optional apply of a

Stand-by potential

after the end of the volt-

age sweep (details see Stand-by potential).


Stirring

If switched on (

Stirrer > 0 rpm

), the solution in the sample vessel at

the 757 VA Computrace Stand is stirred during all preparation
procedure steps until the start of the equilibration time.

Stirrer (rpm)

[ 0...3000 rpm ; 2000 rpm ]

Revolutions per minute of the stirrer.