Waters Spherisorb Columns - Manual (Page 8)

[ Care and Use ManUal ]
Waters Spherisorb Columns 8
Figure 3: Parker Ferrule in a Waters Style Endfitting
Note: A void appears if tubing with a Parker style ferrule is connected to a Waters
style column.
There is only one way to fix this problem: Cut the end of the tubing
with the ferrule, place a new ferrule on the tubing and make a new
connection. Before tightening the screw, make sure that the tubing
bottoms out in the endfitting of the column. Conversely, if tubing
with a Waters ferrule is connected to a column with Parker style
endfitting, the end of the tubing will bottom out before the ferrule
reaches its proper sealing position. This will leave a gap and create a
leak (Figure 4).
Figure 4: Waters Ferrule in a Parker Style Endfitting
Note: The connection leaks if a Waters ferrule is connected to a column with a
Parker style endfitting.
There are two ways to fix the problem:
1. Tighten the screw a bit more. The ferrule moves forward, and reaches
the sealing surface. Do not overtighten since this may end in breaking
the screw.
2. Cut the tubing, replace the ferrule and make a new connection.
Alternatively, replace the conventional compression screw fitting with
an all-in-one PEEK
® fitting (Waters Part Number PSL613315) that
allows resetting of the ferrule depth. (Note that PEEK fittings are not
recommended for normal-phase applications!) Another approach is to
use a Thermo Corporation SLIPFREE
® connector to always ensure the
correct fit.
The fingertight SLIPFREE connectors automatically adjust to fit all
compression screw type fittings without the use of tools (Figure 5).
Figure 5: Single and Double SLIPFREE Connectors
SLIPFREE Connectors Features
• Tubing pushed into endfitting, thereby guaranteeing a void-free
connection
• Connector(s) come(s) installed on tubing
• Various tubing i.d. and lengths available
• Fingertight to 10,000 psi – never needs wrenches
• Readjusts to all column endfittings
• Compatible with all commercially available endfittings
• Unique design separates tube-holding function from sealing function
Table 5. Waters Part Numbers for SLIPFREE Connectors
SLIPFREE Type and
Tubing Length Tubing Internal Diameter
0.005” 0.010” 0.020”
Single 6 cm PSL 618000 PSL 618006 PSL 618012
Single10 cm PSL 618002 PSL 618008 PSL 618014
Single 20 cm PSL 618004 PSL 618010 PSL 618016
Double 6 cm PSL 618001 PSL 618007 PSL 618013
Double 10 cm PSL 618003 PSL 618009 PSL 618015
Double 20 cm PSL 618005 PSL 618001 PSL 618017
Void
Gap