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Waters Biopharmaceutical Training Kit User Manual

Biopharmaceutical training kit, Care and use manual

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[ CARE AND USE MANUAL ]

CONT ENTS

I. INT RODUCTION

II. STANDARD P REPARATION

III. ADDITIONAL RESOURC ES

IV. ORDERING INFORMATION

Biopharmaceutical Training Kit

I. INT RODUCTION

The Biopharmaceutical Training Kit is designed to provide trainers
and customers with high quality standards that can be utilized as a
starting point for running biopharmaceutical applications on their
Waters UPLC inlet with Tof or Q-Tof mass spectrometry detection
systems. The training kit pulls together many of the individual
standard samples that are often used in demos and training classes,
including reference compounds for calibration and lockmass. This
kit provides a foundation for biopharmaceutical LC-MS analysis and
can be used for optimization of methods prior to running valuable
samples to ensure system performance and confidence in results.

Table 1. Kit Components for Biopharmaceutical Training Standards (P/N 186006921)

Part #

Contents

Description of Components Acid

Amount

per Vial

Container

186006921-1

1 x 15 mL

Horse Heart Myoglobin

2.5 mg

15 mL Clear Nalgene Bottle

186006921-2

1 vial

Intact mAb Mass Check Standard

1 mg

TruView™ Max Recovery with non-slit PTFE/
silicone Septa (p/n 186005668CV)

186006921-3

1 vial

Glu-fibrinopeptide B

0.5 mg

4 mL Amber Screw Top Vial

186006921-4

1 vial

MassPREP Enolase Digest

1 nmol

TruView Max Recovery with non-slit PTFE/
silicone Septa (p/n 186005668CV)

186006921-5

1 vial

Reverse Peptide Ser-Asp-Gly-Arg-Gly

1.0 mg of each 4 mL glass amber bottle with screw top

186006921-6

1 vial

Reverse Peptide Gly-Arg-Gly-Asp-Ser

1.0 mg of each 4 mL glass amber bottle with screw top

Table 2. Kit Components for Biopharmaceutical Prep Kit (P/N 186007517)

Part #

Contents

Description of Components Acid

Amount

per Vial

Container

186007517-1

1 x 2 mL

Formic Acid

2 mL

2 mL Ampoule

186007517-2

1 x 30 mL

Sodium Cesium Iodide

2 μg/μL

30 mL Nalgene

290002010

3

30 mL Nalgene Fludics Bottle (with cap)

Empty

30 mL Nalgene Fludics Bottle (with cap)

The Biopharmaceutical Training Kit comes in two separate boxes. The Biopharmaceutical Training Standard Kit (see Table 1) contains
the standards. This kit is shipped at ambient temperatures, however upon receipt of this kit, please store at -20 °C to maximize long
term stability. The Biopharmaceutical Training Prep Kit (see Table 2) contains the materials needed for solubilization and standard prep.
This kit is shipped at ambient temperatures and can be stored at room temperature. Once any component is opened, use right away for
optimum results.