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Metrohm 743 Rancimat User Manual

Page 5

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Table of contents

743 Rancimat

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III

Table of contents

1 Introduction

1

1.1

Instrument description ......................................................... 1

1.2

Rancimat method ................................................................. 2

1.3

About the documentation ................................................... 3

1.3.1

Symbols and conventions ........................................................ 3

1.4

Safety instructions ................................................................ 4

1.4.1

General notes on safety ........................................................... 4

1.4.2

Electrical safety ........................................................................ 5

1.4.3

Flammable solvents and chemicals ........................................... 6

1.4.4

Recycling and disposal ............................................................. 6

2 Overview of the instrument

7

3 Installation

10

3.1

Setting up the instrument .................................................. 10

3.1.1

Packaging .............................................................................. 10

3.1.2

Checks .................................................................................. 10

3.1.3

Location ................................................................................ 10

3.2

Mounting accessories ......................................................... 10

3.2.1

Mounting accessories for the internal air supply ..................... 10

3.2.2

Mounting accessories for the external air supply .................... 13

3.2.3

Equipping the reaction and measuring vessels ........................ 13

3.2.4

Inserting vessels / Establishing tubing connections ................. 16

3.2.5

Mounting the exhaust collection tube (optional accessories) . . 17

3.3

Mains connection ............................................................... 18

3.3.1

Checking the mains voltage ................................................... 18

3.3.2

Replacing fuses ...................................................................... 18

3.3.3

Mains cable and mains connection ........................................ 19

3.3.4

Switching the instrument on/off ............................................ 19

3.4

Connecting a PC ................................................................. 19

3.4.1

Connecting the 743 Rancimat and the PC .............................. 19

3.4.2

Installing the software ........................................................... 20

3.4.3

Carrying out basic settings ..................................................... 22

4 Operation

24

4.1

Fundamentals of operation ............................................... 24

4.1.1

Starting and exiting the program ........................................... 24

4.1.2

Terms .................................................................................... 25

4.1.3

Control window .................................................................... 25

4.1.4

Results window ..................................................................... 27

4.1.5

File types ............................................................................... 30

4.1.6

Context-sensitive menus ........................................................ 31