Metrohm 820 IC Separation Center - Manual (Page 5)

Table of contents
819 IC Detector / 820 IC Separation Center
I
Table of contents
1 Introduction.................................................... 1
1.1 Instrument description ............................................................. 1
1.1.1 819 IC Detector .............................................................................1
1.1.2 820 IC Separation Center..............................................................2
1.1.3 Schematic arrangement of the IC systems...................................3
1.2 Parts and controls .................................................................... 4
1.2.1 819 IC Detector .............................................................................4
1.2.2 820 IC Separation Center..............................................................6
1.3 Information on the Instructions for Use ................................ 10
1.3.1 Organization ................................................................................10
1.3.2 Notation and pictograms ............................................................11
1.4 Safety notes ............................................................................ 12
1.4.1 General precautionary rules........................................................12
2 Installation ................................................... 13
2.1 Setting up the instrument ....................................................... 13
2.1.1 Packaging....................................................................................13
2.1.2 Check...........................................................................................13
2.1.3 Location.......................................................................................13
2.1.4 Arrangement of the instruments..................................................13
2.2 Installation of accessories ..................................................... 15
2.2.1 Insert detector block....................................................................15
2.2.2 Connection of column heating....................................................18
2.2.3 Connection of syringe and aspirating tubing..............................19
2.2.4 Connection of the drain tube.......................................................19
2.2.5 Connection of the 6.5324.000 Bottle rack (option).....................19
2.3 Electrical connection .............................................................. 20
2.3.1 Connection to 830 IC Interface ...................................................20
2.3.2 Connection to PC ........................................................................23
2.4 Mains connection.................................................................... 25
2.4.1 819 IC Detector ...........................................................................25
2.4.2 820 IC Separation Center............................................................27
2.4.3 Column heating ...........................................................................27
2.5 Software-installation............................................................... 27
2.6 Capillary connections............................................................. 28
2.7 Connection of 818 IC Pump ................................................... 29
2.7.1 Electrical connection ...................................................................29
2.7.2 Pulsation dampener ....................................................................29
2.7.3 Filter unit PEEK............................................................................30
2.7.4 Connection to injection valve ......................................................31
2.8 Precolumns ............................................................................. 33
2.9 Separating columns and suppressor module....................... 34
2.9.1 General information on separating columns ..............................34
2.9.2 Installing a separating column in the column heating................35
2.9.3 Selection of the sample loop ......................................................37
2.9.4 General information on suppressor module...............................37
2.9.5 One-channel system without suppressor module......................39
2.9.6 Two-channel system without suppressor module......................41
2.9.7 One-channel system with suppressor module ...........................42
2.9.8 Two-channel system with suppressor module ...........................47
2.9.9 Leak testing and conditioning.....................................................48