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Relative viscosity calculation, Software selection of blank, Procedure for blank definition – Cannon Instrument miniPV-X User Manual

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CANNON

®

miniPV-Series Automatic Viscometer with VISCPRO

®

Instruction & Operation Manual

Version 1.a— January, 2011;

CANNON

®

Instrument Company

2139 High Tech Road • State College, PA 16803 • USA

22

*The term absolute viscosity, as used in this manual, is also known as
dynamic viscosity. For the purpose of VISCPRO® software viscosity

calculations, and per ASTM D 2857 specifications, the absolute viscosity

is defined by the equation ç = Ctñ - Eñ/t 2 where C is a constant, t is the

drop time, ñ is the solution or solvent density and E is the kinetic energy

correction constant.

Relative viscosity calculation

The relative viscosity (RV) ratio (solute to solvent blank) is therefore defined
by the equation:

Software selection of blank

Since determination of a relative viscosity involves a comparison of solution
and blank, the VISCPRO controlling software requires the identification of a
blank for any samples tested using the Determine Solution Relative Viscosity
sample action. The blank is ordinarily selected from a list of solvents main-
tained by the VISCPRO database. This list is accessible from the Polymer
Measurement Sample Options window by using the drop-down list feature:

To display the list, click on the arrow. If the correct blank has not yet been
defined, the user may create a new blank by typing an ID for the blank into the
open field in the Polymer Measurement Sample Options window:

Procedure for blank definition

New blanks are created by testing the solvent in the miniPV using the
Determine Solvent Viscosity sample action. Follow the procedure for

testing samples

1. Select Determine Solvent Viscosity as the sample action for the

desired sample.

2. Enter an ID for each blank that includes both a description of the

blank and also the temperature at which that blank is to be tested in

the miniPV. The blank must be tested at the same temperature

intended for the solution

NOTE

In some MiniPV applications involving dilute solutions, it may not be

necessary to input the density for the solvent blank and/or solution. If you

choose not to input solvent density for either the blank or for the sample,