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Phenol – LaMotte SMART 2 User Manual

Page 217

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PHENOL

AMINOANTIPYRINE METHOD • CODE 3652-SC

QUANTITY

CONTENTS

CODE

5 g

Aminoantipyrine Reagent

7825-C

30 mL

*Ammonium Hydroxide Solution

*7826-G

2 x 60 mL

*Potassium Ferricyanide Solution

*7827-H

1

Spoon, 0.1 g, plastic

0699

1

Pipet, plain, plastic

0352

1

Pipet, 1.0 mL, plastic

0354

*WARNING: Reagents marked with an * are considered to be potential health
hazards. To view or print a Material Safety Data Sheet (MSDS) for these reagents go to
www.lamotte.com. To obtain a printed copy, contact LaMotte by e-mail, phone or fax.

Phenols may occur in domestic and industrial waste waters and in drinking
water supplies. Chlorination of waters containing phenols may produce
odiferous and objectionable tasting chlorophenols. Natural waters sedom
contain more than 1 mg/L phenol.

APPLICATION:

Drinking and surface waters; domestic and industrial waste
water.

RANGE:

0.00–6.00 ppm Phenol

METHOD:

4-Aminoantipyrine is oxidized in the presence of all ortho-
and meta- substituted phenols to form a colored complex in
proportion to the amount of phenol present.

SAMPLE
HANDLING &
PRESERVATION:

Phenols are subject to biological and chemical oxidation.
Samples should be analyzed within 4 hours after collection.
If sample cannot be analyzed within 4 hours, it can be
preserved by acidification with phosphoric acid to pH 4.0.

INTERFERENCES:

Oxidizing and reducing chemicals, alkaline pH values, and
phenol decomposing bacteria may interfere with the test.

Smart2 TEST PROCEDURES 12.07

Phenol 1/2