Metrohm 763 PVC Thermomat Manual - Manual (Page 18)

2.2 Attaching the accessories
763 PVC Thermomat
11
• Place reaction vessel cover 22 on reaction vessel 11.
• Connect the white connecting tubing 33 to connection 31 31 of
reaction vessel cover 22 (see Fig. 3).
4 Inserting the reaction vessel into the instrument
• Place the sample in the reaction vessel (see section 4.6.2).
• When the required temperature has been reached insert
reaction vessel 11 with attached reaction vessel cover 22 in the
openings provided for it on the 763 PVC Thermomat.
5 Making the tubing connections
• Connect the white connecting tubing 3 3 attached to reaction
vessel cover 22 to connection piece 22 22 of measuring vessel
cover 55.
• Screw one end of brown connecting tubing 66 to connection
nipple 30 30 of reaction vessel cover 22.
• Screw the other end of brown connecting tubing 66 to the
corresponding connection 19 19 on the 763 PVC Thermomat
(see Fig. 3).
The 6.1428.020 transparent glass measuring vessel
available as an option can be used instead of the
6.1428.100 polycarbonate measuring vessel; in
contrast to the polycarbonate vessel this can be
cleaned with acetone.
2.2.3 Exhaust collection tube (option)
For selective exhaust lead off the 6.2757.000 Exhaust collection
tube available as an option can be fitted to the 763 PVC Thermomat. In
addition to the exhaust collection tube 8 x 6.1816.010 Silicone tubing
(22 cm) must also be ordered. Attach the exhaust collection tube as
described below:
1 Positioning the exhaust collection tube
• Place the exhaust collection tube with the two supports in the
two mountings 21 21 (see Fig. 3) on the 763 PVC Thermomat so
that the connection for leading off the exhaust is located to
the rear.
2 Connecting the measuring vessel
• Screw a connection piece 22 22 into opening 23 23 of the measur-
ing vessel cover 55.