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Summary of quality assurance checks, 8 summary of quality assurance checks -21, Able – Teledyne 6200A - Sulfides analyzer User Manual

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TAI Model 6200A SO

2

Analyzer Operator Manual, 02164, Rev. G

7.8.8 Summary of Quality Assurance Checks

The following items should be checked on a regularly scheduled basis to assure high quality data
from the 6200A. See Table 7-14 for a summary of activities also the QA Handbook should be
checked for specific procedures.

Table 7-14: Activity Matrix

Characteristic

Acceptance limits

Frequency and method
of measurement

Action if requirements
are not met

Shelter temperature

Mean temperature
between 22

o

C and

28

o

C (72

o

and 82

o

F),

daily fluctuations
not greater than
±2

o

C

Check thermograph
chart weekly for
variations greater than
±2

o

C (4

o

F)

1. Mark strip chart for

the affected time
period

2. Repair or adjust

temperature control

Sample introduction
system

No moisture, foreign
material, leaks,
obstructions; sample
line connected to
manifold

Weekly visual inspection Clean, repair, or replace

as needed

Recorder

1. Adequate ink &

paper

2. Legible ink traces

3. Correct chart

speed and range

4. Correct time

Weekly visual inspection 1. Replenish ink and

paper supply

2. Adjust time to agree

with clock; note on
chart

Analyzer operational
settings

1. TEST

measurements at
nominal values

2. 2. 6200A in

SAMPLE mode

Weekly visual inspection Adjust or repair as

needed

Analyzer operational
check

Zero and span within
tolerance limits as
described in Subsec.
9.1.3 of Sec. 2.0.9
(Q.A. Handbook)

Level 1 zero/span every
2 weeks; Level 2
between Level 1 checks
at frequency desired
analyzer by user

1. Find source of error

and repair

2. After corrective

action, re-calibrate
analyzer

Precision check

Assess precision as
described in Sec.
2.0.8 and Subsec.
3.4.3 (Ibid.)

Every 2 weeks, Subsec.
3.4.3 (Ibid.)

Calc, report precision,
Sec. 2.0.8 (Ibid.)

7-21