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Waters Sep-Pak DNPH-Silica Cartridges User Manual

Care and use manual, Waters sep-pak dnph-silica cartridge

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[ Care and Use ManUal ]

Waters Sep-Pak DNPH-Silica Cartridge

1

Contents

I. IntroduCtIon

a. Sep-Pak DNPH-Silica Cartridge Description

II. usInG seP-PAK dnPH CArtrIdGes

a. Theory of Operation

b. Preventing Contamination
c. Collecting the Sample
d. Eluting the Derivatives

III. AnALYZInG tHe dnPH derIVAtIVes

a. Operating Guidelines

b. Performing HPLC Analysis
c. Analyzing a Cartridge Blank
d. Selecting Separation Conditions

IV. APPLICAtIon eXAMPLes

a. Estimating Sample Volume

b. Analysis of Auto Exhaust Emissions
c. Analysis of Residential Air
d. Analysis of Research Lab Air

V. storAGe And dIsPosAL oF used CArtrIdGes

VI. trouBLesHootInG

VII. reFerenCes And BIBLIoGrAPHY

VIII. orderInG InForMAtIon APPendICes

IX. APPendICes

a. Measuring Acetonitrile Purity
b. Synthesizing DNPH Derivative Standards
c. Measuring Sample Breakthrough

I. IntroduCtIon

Waters Sep-Pak

®

DNPH-Silica cartridges are convenient, reproducible

sampling devices for quantifying aldehydes and ketones in gasses,
including air within a range of 1 to 5,000 parts per billion (ppbv).

WAters seP-PAK dnPH-sILICA CArtrIdGe