beautypg.com

Brookfield R/S Coaxial Cylinder Rheometer User Manual

Page 68

background image

Brookfi eld Engineering Labs., Inc.

Page 68

Manual No. M08-219-B1211

D.1.4

Editing and Running Programs

As detailed in the R/S Rheometer operation manual, stand-alone programs can be written
under the Section VI.6.2: Utilities

Edit Programs menu for the R/S-SST+ to facilitate fast

test turnaround.

The two test methods that are most often used to evaluate soft solids with the R/S-SST+ are the
Constant Rate Test and the Creep Test.

D.2.1

The Constant Rate Test

For products like: Stiff pastes, slurries, set gels, waxes.

Properties measured: Yield stress or torque, equilibrium stress strain at yield, rigidity
modulus.

Description: In the constant rate test, the vane is rotated at a constant low rotational rate (typically
0.1 to 0.5 rpm) and the torque or stress is measured against time, rotational angle or strain.

Example method: Constant rotation at 0.2 rpm, linear data collection, 60 data points over 60
seconds. A V30-15 vane (30 mm high by 15 mm across) is used in an open confi guration (see
Section D.3.3: Setting Up Vanes).

Figure D-3

D.2 Getting Started in Soft Solids Testing