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Trivalent chromium procedure – LaMotte SMART3 Colorimeter User Manual

Page 136

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6. Remove

fl ask from heat. Cool sample under running water. This is the digested

sample.

7. Pour digested sample into clean graduated cylinder (0418). Dilute to the 50 mL

line with Deionized Water (5115).

8. Press and hold

until colorimeter turns on.

9. Press

ENTER

to select TESTING MENU.

10. Select ALL TESTS or another sequence containing 021 Chromium) from

TESTING MENU.

11. Scroll to and select 021 Chromium from menu.
12. Rinse a clean tube (0290) with sample water. Fill to 10 mL line with sample

water.

13. Insert tube into chamber, close lid and select SCAN BLANK.
14. Remove tube from colorimeter. Use 0.1 g spoon (0699) to add one level

measure of *Chromium Reagent Powder (V-6276). Cap and shake for one

minute. Wait 3 minutes.

15. During the waiting period, fold a piece of fi lter paper in half, then in half again to

form a cone. Push corners together to open end, and insert into funnel (0459).

16. Filter sample into a clean tube (0290). Cap and mix. Insert tube of fi ltered

sample into chamber, close lid and select SCAN SAMPLE. Record result.

17. Press

to turn colorimeter off or press

EXIT

to exit to a previous menu or

make another menu selection.

TRIVALENT CHROMIUM PROCEDURE

Subtract hexavalent chromium from total chromium. Record as ppm trivalent

chromium.

Trivalent Chromium = Total Chromium – Hexavalent Chromium

CHROMIUM, Hexavalent, Trivalent, Total

SMART3 Test Procedures 11.10

Test P

rocedures