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Metrohm NIRS XDS RapidLiquid Analyzer User Manual

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Table of contents

1

Introduction ................................................................................................................... 5

2

Site Readiness ................................................................................................................ 7

2.1

Temperature and Humidity ........................................................................... 7

2.2

General Environment .................................................................................... 7

2.3

Electrical Power ............................................................................................ 7

2.4

Vibration ....................................................................................................... 7

2.5

Instrument Communication .......................................................................... 7

2.6

Instrument Dimensions and Weight .............................................................. 8

3

XDS Instrument Connection ........................................................................................... 9

3.1

Network Connection, connected to an active network port as shown .......... 9

3.2

Direct Connection, in a free-standing manner with no network connection

10

3.3

Overview of XDS Instrument Communication ............................................. 10

3.4

Flowchart Diagram of XDS Communication Protocol .................................. 11

3.4.1

Network Evolution Issues ...................................................................................... 12

3.4.2

Quick Glossary of Terms: ....................................................................................... 12

3.5

Connection in Vision ................................................................................... 13

3.6

Troubleshooting Connection Problems ....................................................... 14

3.6.1

Network Troubleshooting Overview ...................................................................... 15

3.6.2

Direct Connection Troubleshooting Overview ........................................................ 19

4

Assembly of the Instrument ......................................................................................... 20

5

Rapid Liquid Module .................................................................................................... 25

5.1

Wavelength Calibration of the Rapid Liquid Analyzer ................................. 25

5.2

Blank Correction ......................................................................................... 25

5.3

Cuvette Types ............................................................................................. 26

5.4

Flow-Through Fittings ................................................................................ 26

5.5

Cuvette Lifting Handle ................................................................................ 27

5.6

Cuvette Spacers .......................................................................................... 27

5.7

Temperature Control Information ............................................................... 27

5.8

Instructions for closing the sample drawer using Vision ............................. 28

5.9

Liquid Sampling Considerations .................................................................. 28

6

Vision Software: Connection to the Instrument ............................................................ 30

7

Instrument Diagnostics................................................................................................. 35

7.1

Setup Diagnostics ....................................................................................... 35

7.1.1

Instrument Identification ....................................................................................... 36

7.1.2

Wavelength Linearization ...................................................................................... 36

7.1.3

Blank Correction ................................................................................................... 38

7.1.4

Instrument Calibration .......................................................................................... 39

7.1.5

IPV Setup (Instrument Performance Verification) ................................................... 44

7.2

Evaluation Diagnostics ................................................................................ 46

7.2.1

Wavelength Certification ...................................................................................... 46