2 control with «ic cap» (automated operation), Control with «ic cap» (automated operation) – Metrohm 761 SD Compact IC User Manual
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5 Operation
761 SD Compact IC / Instructions for Use 8.
761.1043
86
5.2.2
Control with «IC Cap» (automated operation)
Start the «IC Cap» software and log in (see Section 2.12.4).
Configuration
auto.cfg
should have been installed during installation
(see Section 2.12.2). If not, now load configuration
auto.cfg
(see Sec-
With automated sample change, it is possible to predefine the se-
quence of conditioning, calibration and sample determination with a
sample table (queue).
5.2.2.1
Preparing sample vessels (automated operation / «IC Cap»)
1 Prepare calibration standards
⇒
Fill each of the 6 sample vessels with an MCAL standard
(150, 250, 350, 450, 550 and 650 mg/L H
3
PO
4
plus basic con-
tent of nitrate and sulfate) and position them at the required
position in the sample rack of the 766 IC Sample Processor.
The MCAL standard bottles are supplied as accessories
(6.2321.000).
2 Prepare the samples
⇒
Fill sample vessels with the samples to be measured and po-
sition them at the required position in the sample rack.
3 Prepare the rinsing solution
⇒
Fill the special beakers at the rinsing position of the 766 IC
Sample Processor with ultra-pure water.
5.2.2.2
Creating a sample table (automated operation / «IC Cap»)
⇒
After opening «IC Cap», the sample table (queue) should be dis-
played at the left-hand side of the screen (if configuration
auto.cfg
is
loaded).
⇒
Create the sample table (see Administrator Manual «IC Cap 2.0»,
Section 2.3). First perform a conditioning step with system
startup.smt
. Then perform the calibration measurements and the
sample determinations with the system
auto.smt
. Assign the number
for
Vial
to the rack positions you have selected.