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Ic net, Ic cap, Operation – Metrohm 761 SD Compact IC User Manual

Page 6

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Table of contents

761 SD Compact IC / Instructions for Use 8.

761.1043

II

2.12

Connection to the PC ................................................................................30

2.12.1

Connecting cable 6.2134.100.......................................................................... 30

2.12.2

Software installation ......................................................................................... 30

2.12.3

Basic settings «IC Net»..................................................................................... 31

2.12.4

Basic settings «IC Cap» ................................................................................... 33

2.13

Deaerating the pump and rinsing the pulsation dampener ....................34

2.13.1

Deaerating the pump ....................................................................................... 34

2.13.2

Rinsing the pulsation dampener...................................................................... 35

2.14

Rinsing before fitting the column .............................................................37

2.15

Precolumn and separating column ..........................................................39

2.15.1

Metrosep RP Guard ......................................................................................... 39

2.15.2

Metrosep A Supp 1 HS separating column..................................................... 40

2.16

Attaching tubing to side panels................................................................42

3

«IC Net» ..................................................................... 43

3.1

«IC Net» – User interface for the 761 SD Compact IC..............................43

3.1.1

Systems - Methods .......................................................................................... 43

3.1.2

Opening a system ............................................................................................ 43

3.1.3

Opening a method ........................................................................................... 44

3.1.4

Connect a system ............................................................................................ 44

3.1.5

Instrument icon................................................................................................. 45

3.1.6

System parameters for linked system ............................................................. 45

3.1.7

Hardware settings ............................................................................................ 50

3.2

Systems supplied ......................................................................................54

3.2.1

System "startup.smt" ........................................................................................ 54

3.2.2

System "manual.smt"........................................................................................ 55

3.2.3

System "auto.smt" ............................................................................................ 56

3.2.4

System "shutdown.smt".................................................................................... 61

4

«IC Cap» .................................................................... 64

4.1

«IC Cap» introduction ................................................................................64

4.1.1

Login................................................................................................................. 64

4.1.2

User interface ................................................................................................... 64

4.2

«IC Cap» - Configuration ...........................................................................66

4.2.1

Predefined configurations................................................................................ 66

4.2.2

Configuration "manual.cfg"............................................................................... 66

4.2.3

Configuration "auto.cfg" ................................................................................... 72

5

Operation .................................................................. 77

5.1

Operation with manual sample change....................................................77

5.1.1

Control with «IC Net» (manual operation) ........................................................ 77

5.1.2

Control with «IC Cap» (manual operation) ....................................................... 81

5.2

Operation with automated sample change ..............................................84

5.2.1

Control with «IC Net» (automated operation)................................................... 84

5.2.2

Control with «IC Cap» (automated operation) ................................................. 86

6

Notes – Maintenance – Faults .................................. 88

6.1

Practical notes on ion chromatography ...................................................88

6.1.1

Separating columns ......................................................................................... 88

6.1.2

High-pressure pump ........................................................................................ 88

6.1.3

Eluents.............................................................................................................. 89

6.1.4

Peristaltic pump................................................................................................ 89

6.1.5

Suppressor module.......................................................................................... 89

6.1.6

Connections ..................................................................................................... 90