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Metrohm 793 IC Sample Preparation Module User Manual

Page 25

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2.4

2.4

2.4

2.4 Connection

Connection

Connection

Connection to

to

to

to aaaa Modular

Modular

Modular

Modular IC

IC

IC

IC System

System

System

System for Cation Elimination

793 IC Sample Prep Module/ 8.793.1003 Instructions for Use

21

7 SP Module A connection 3: H

2

O

x Pull the inlet capillary 28

28

28

28 marked with “H

2

O“ at SP Module A

connection 22

22

22

22 (see Fig. 6) through one of the rear panel

openings 41

41

41

41 or 43

43

43

43 of the 733 IC Separation Center.

x Mount a PEEK compression fitting 31

31

31

31 (6.2744.010) on the

end of inlet capillary 28

28

28

28 and screw this on to the second

PEEK filter unit 36

36

36

36 (6.2821.100) (see Fig. 7).

x Mount coupling 35

35

35

35 on to the inlet of the PEEK filter unit and

push this coupling on to outlet end of the second pump

tubing 33

33

33

33 (see Fig. 7).

x Mount suction tubing: cut a piece of PTFE Tubing 30

30

30

30

(6.1803.020) to the desired length.

x Mount a PEEK compression fitting 31

31

31

31 (6.2744.010) on one

end of PTFE tubing 30

30

30

30 and screw this on to coupling 32

32

32

32..

x Push coupling 32

32

32

32 on to the inlet end of the second pump

tubing 33

33

33

33 (see Fig. 7).

x Immerse the other end of the suction tubing in a vessel con-

taining rinsing solution (normally dist. H

2

O) and fix in place.

x Pull outlet capillary 27

27

27

27 marked with “Waste“ at SP Module A

connection 22

22

22

22 (see Fig. 6) through one of the rear panel

openings 41

41

41

41 or 43

43

43

43 of the IC Separation Center 733.

x Lead outlet capillary 27

27

27

27 to a sufficiently large waste container

and fix in place.

8 Startup of 793 IC Sample Prep Module

x Set switch 2

222 to "OFF".

x Switch on 793 IC Sample Prep Module with mains switch 13

13

13

13

and set switch 3

333 to "ON".

x Adjust the contact pressure for both tubing cartridges: press

contact pressure lever 5

555 upwards until the solutions just start

to be drawn in. Then press the contact pressure lever

upwards until it clicks once more to obtain optimal contact

pressure.

x Check all tubing from the storage vessels through the tubing

cartridges and the SP Module A up to the waste containers

for leakage of liquids. If liquid escapes anywhere the

corresponding compression fitting must be tightened further

or changed.

x Before using the SP Module A for sample pretreatment, its

cation exchange material should be conditioned. Inject 30%

sodium hydroxide 15 times (five injections per unit) using the

sample program of the system “Neutralization” as described

in the following section. The run time can be 20 min. each

while the separation column doesn’t have to be installed.

Pump tubings are consumable material with a lifetime which depends

on the contact pressure. This is why the tubing cartridges should be

raised completely by loosening snap-action lever

10

10

10

10

on the right-hand

side if the pump is to remain switched off for a considerable length of

time (the set contact pressure remains unchanged).