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Metrohm 850 Professional IC MSM-HC MCS Prep 3 User Manual

Page 7

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Table of contents

850 Professional IC Anion – MSM-HC – MCS – Prep 3

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V

5.3

Door ..................................................................................... 81

5.4

Eluent ................................................................................... 81

5.4.1

Production ............................................................................. 81

5.4.2

Operation .............................................................................. 82

5.5

High pressure pump ........................................................... 82

5.5.1

Protection .............................................................................. 82

5.5.2

Maintenance ......................................................................... 83

5.6

Inline filter ........................................................................... 93

5.6.1

Maintenance ......................................................................... 93

5.7

Inline sample preparation .................................................. 95

5.8

Rinsing the sample path .................................................... 95

5.9

Sample degasser ................................................................. 97

5.9.1

Operation .............................................................................. 97

5.10 Sample preparation module (SPM) ................................... 97
5.10.1

Protection .............................................................................. 97

5.10.2

Operation .............................................................................. 97

5.10.3

Maintenance ......................................................................... 98

5.11 Peristaltic pump ................................................................ 103
5.11.1

Operation ............................................................................ 103

5.11.2

Maintenance ....................................................................... 103

5.12 Injection valve .................................................................. 105
5.12.1

Protection ............................................................................ 105

5.13 High Capacity Metrohm Suppressor Module

(MSM-HC) .......................................................................... 106

5.13.1

Protection ............................................................................ 106

5.13.2

Operation ............................................................................ 106

5.13.3

Maintenance ....................................................................... 107

5.14 Metrohm CO

2

suppressor (MCS) ..................................... 112

5.14.1

Replacing the CO

2

adsorption cartridge ............................... 112

5.14.2

Regenerating the H

2

O adsorption cartridge .......................... 112

5.15 Conductivity detector ....................................................... 113
5.15.1

Maintenance ....................................................................... 113

5.16 Separation column ........................................................... 113
5.16.1

Separating efficiency ............................................................ 113

5.16.2

Protection ............................................................................ 114

5.16.3

Storage ............................................................................... 114

5.16.4

Regeneration ....................................................................... 114

5.17 Quality Management and validation with Metrohm .... 115

6 Troubleshooting

116

6.1

Problems and their solutions .......................................... 116