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3 operation, 3operation, 1 handling the suppressor – Metrohm 753 Suppressor Module User Manual

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3.1 Handling the suppressor

753 Suppressor Module / 8.753.1003 Instructions for Use

19

3

Operation

3.1

Handling the suppressor

General

The Metrohm Suppressor Module MSM for chemical suppression

installed in the suppressor block consists of a total of 3 suppressor

units which are in turn used for suppression, regenerated with sulfuric

acid and rinsed with water. In order to record each new chromatogram

under comparable conditions a freshly regenerated suppressor unit is

normally used. Switching is either carried out automatically together

with valve switching or manually.

Correct connections

The three inlets and outlets numbered 1...3 on the suppressor each

have 2 permanently mounted PTFE capillaries, which must be con-

nected as described in sections 2.3.2 or 2.4.2 respectively (see Fig. 6).

Flow direction

The suppressor units must never be regenerated with H

2

SO

4

in the

same flow direction used for the eluent. You should thus always install

the inlet and outlet capillaries as described in sections 2.3.2 or 2.4.2

respectively according to the scheme shown in Fig. 6.

Never switch when dry

The suppressor must never be switched in the dry state as there is a

danger of blocking.

No recycling

The recycling process (returning the eluent to the storage vessel)

must not be carried out when the suppressor is in operation.