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Metrohm 753 Suppressor Module User Manual

Page 21

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2 Installation

753 Suppressor Module / 8.753.1003 Instructions for Use

18

11 Suppressor connection 3: H

2

O

Pull the inlet capillary 28

28 marked with “H

2

O“ at suppressor

connection 22

22 (see Fig. 6) through one of the rear panel

openings 41

41 or 43

43 of the 733 IC Separation Center.

Mount a PEEK compression fitting 31

31 (6.2744.010) on the

end of inlet capillary 28

28 and screw this on to coupling 32

32

(6.2744.030) (see Fig. 7).

Push coupling 32

32 on to the outlet end of the second pump

tubing 33

33 (see Fig. 7).

Mount suction tubing: cut a piece of PTFE Tubing 30

30

(6.1803.020) to the desired length.

Mount a PEEK compression fitting 31

31 (6.2744.010) on one

end of PTFE tubing 30

30 and screw this on to coupling 32

32 (see

Fig. 7).

Push coupling 32

32 on to the inlet end of the second pump

tubing 33

33 (see Fig. 7).

Immerse the other end of the suction tubing in a vessel

containing rinsing solution (normally dist. H

2

O) and fix in

place.

Pull outlet capillary 27

27 marked with “Waste“ at suppressor

connection 22

22 (see Fig. 6) through one of the rear panel

openings 41

41 or 43

43 of the IC Separation Center 733.

Lead outlet capillary 27

27 to a sufficiently large waste container

and fix in place.

12 Startup of 753 Suppressor Module

Set switch 22 to "OFF".

Switch on 753 Suppressor Module with mains switch 13

13 and

set switch 33 to "ON".

Adjust the contact pressure for both tubing cartridges: press

contact pressure lever 55 upwards until the solutions just start

to be drawn in. Then press the contact pressure lever up-

wards until it clicks once more to obtain optimal contact pres-

sure.

Before switching the suppressor to the next position for the

first time rinse all three suppressor units with solution for

5 min.

Check all tubing from the storage vessels through the tubing

cartridges and the suppressor up to the waste containers for

leakage of liquids. If liquid escapes anywhere the corre-

sponding compression fitting must be tightened further or

changed.

Pump tubings are consumable material with a lifetime which depends

on the contact pressure. This is why the tubing cartridges should be

raised completely by loosening snap-action lever 10

10 on the right-hand

side if the pump is to remain switched off for a considerable length of

time (the set contact pressure remains unchanged).