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Methods optimization – Hanna Instruments HI 903 User Manual

Page 130

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9-2

METHODS OPTIMIZATION

9.2.4 Liquid Samples ........................................................................................ 9 - 1 1

9.2.5 Sample Preparation Techniques ................................................................... 9 - 1 2

9.2.5.1 Internal Extractions .........................................................................................9 - 1 2

9.2.5.2 Dilutions ..........................................................................................................9 - 1 2

9.2.5.3 External Dissolution .........................................................................................9 - 1 3

9.2.5.4 External Extractions .........................................................................................9 - 1 3

9.2.5.5 Homogenization ..............................................................................................9 - 1 4

9.2.5.6 Heating...........................................................................................................9 - 1 4

9.3

Karl Fischer Reagent System ................................................................ 9-15

9.3.1 Reagent System Classification ................................................................... 9 - 1 5

9.3.1.1 One-Component Reagent Systems .................................................................. 9 - 1 5

9.3.1.2 Two-Component Reagent Systems .................................................................. 9 - 1 5

9.3.1.3 Reagents for Aldehydes and Ketones ............................................................... 9 - 1 5

9.3.2 Choosing and Modifying a Solvent ............................................................... 9 - 1 6

9.3.3 Water Standards ......................................................................................... 9 - 1 6

9.3.4 Standardizing the Titrant ............................................................................. 9 - 1 7