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4 ph calibration, Ph calibration – Xylem handylab multi 12 User Manual

Page 22

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Operation

handylab multi 12

22

ba75371e03

11/2009

4.2.4

pH calibration

Why calibrate?

pH electrodes age. This changes the asymmetry (zero point) and slope of the
pH electrode. As a result, an inexact measured value is displayed. Calibration
determines the current values of the asymmetry and slope of the electrode
and stores them in the measuring instrument. Thus, you should calibrate at
regular intervals.

When to calibrate?

z After connecting another electrode
z When the sensor symbol flashes:

– after the calibration interval has expired

– after a voltage interruption, e. g. after changing the batteries

AutoCal TEC

is specially matched to the SI Analytics technical buffer solutions as a fully
automatic two-point calibration. The buffer solutions are automatically rec-
ognized by the measuring instrument. Depending on the instrument setting
(see section 4.8 C

ONFIGURATION

), the instrument displays the relevant buffer

nominal value or the current electrode voltage in mV. The calibration can be
terminated after the first buffer solution. This corresponds to a single-point
calibration
. To do this, the instrument uses the Nernst slope (-59.2 mV/pH
at 25 °C) and determines the asymmetry of the electrode.

AutoRead

The calibration procedure automatically activates the AutoRead function.
The current AutoRead measurement can be terminated at any time (accept-
ing the current value) by pressing .

Displaying the

calibration data

You can view the data of the last calibration on the display. The proceeding
is described on page 50.

Printing the

calibration

protocol

The calibration record contains the calibration data of the current calibration.
You can transmit the calibration protocol to a printer via the serial interface
(see O

UTPUTTING

THE

CALIBRATION

PROTOCOL

ON

THE

INTERFACE

, page 52).

Note
You can automatically print a calibration record after the calibration. To do so,
connect a printer to the interface according to section 4.7.2 before calibrating.
After a valid calibration, the record is printed.