Parr Instrument 6300 - Manual (Page 4)

P a r r I n s t r u m e n t C o m p a n y
T
ABLE OF
C
ONTENTS
4
A
PPENDIX
B
C
ALCULATIONS
— 71
Calculating the Heat of Combustion — 71
General Calculations — 71
Thermochemical Corrections — 71
Fuse Correction — 73
Acid and Sulfur Corrections — 73
ASTM Treatment for Acid and Sulfur — 74
ISO Calculations — 75
Spiking Samples — 75
Conversion to Net Heat of Combustion — 75
A
PPENDIX
C
S
TANDARDIZATION
— 77
Standardizing the Calorimeter — 77
Standard Materials — 77
Automatic Statistical Calculations — 77
A
PPENDIX
D
C
OMMUNICATIONS
I
NTERFACES
— 81
USB Port — 81
Balance and Port Input Driver Specifications — 81
Mettler 011/012 Balance Interface — 81
Sartorius Balance Interface — 81
Generic Interface — 82
Ethernet Interface — 83
Samba Server Feature (Optional) — 84
Bar Code Port — 92
Network Data Services — 92
A
PPENDIX
E
T
ECHNICAL
S
ERVICE
— 93
Return for Repair — 93
A
PPENDIX
F
P
ARTS
L
ISTS
& D
RAWINGS
— 95
Principal Assemblies in Calorimeter — 95
A1250DD2 Controller Assembly — 96
A1251DD Oxygen Solenoid Assembly — 96
A1252DD Water Solenoid Assembly — 96
A1257DD Water Regulator Assembly — 97
A1258DD Temperature Control Assembly — 97
A1260DD Water Level Assembly — 97
A1264DD Air Can Assembly — 98
A1267DD Accessory/Installation Kit — 99
A1265DD Bucket and Stirrer Tube Assembly — 99
6300 Stirrer Motor and Drive — 100
A1255DD Bucket Stirrer Assembly — 100
A1266DD Cover Assembly — 100
6309B Spare Parts Kit — 101
1136 and 1136CL Oxygen Bomb — 103
1138 and 1138CL Oxygen Bomb — 105
F
IGURES
Figure 2-1
Swagelok Tube Fittings — 15
Figure 2-2
6300 Calorimeter Back Panel — 16
Figure 2-3
Closed Loop Configuration with 6520A — 17
Figure 2-4
Closed Loop Configuration with 1564 — 17
Figure 2-5
Open Loop Configuration with 1552 — 18
Figure 2-6
Open Loop Configuration — 18
Figure 4-1
6300 Factory Default Settings — 24
Figure 5-1
Fill Flow Diagram — 28
Figure 5-2
Cotton Thread Assembly — 29
Figure 5-3
Pre-period/Post-period — 30
Figure 5-4
Rinse & Cool Flow Diagram — 32
Figure 5-5
Drain Flow Diagram — 34
Figure 5-6
Combustion Capsule with Adhesive Tape Seal — 37
Figure F-1
Parts Diagram for the 1136 and 1136CL Oxygen
Bombs — 102
T
ABLES
Table B-1
Settings for ISO & BSI Methods — 74
Table C-1
Calorimeter Control Limit Values in J/g When
Benzoic Acid is Used as a Test Sample — 78
Table C-2
Calorimeter Control Limit Values in cal/g When
Benzoic Acid is Used as a Test Sample — 79
Table C-3
Calorimeter Control Limit Values in BTU/lb When
Benzoic Acid is Used as a Test Sample — 80
Table D-1
6300 Data File Naming Convention — 82
Table D-2
6300 Calorimeter Run Data Template — 82
A
PPENDIX
G
B
OMB
R
INSE
C
ONTAINER
A
SSEMBLY
— 127
Overview — 127
Concept of Operation — 127
Connection — 127
Operation — 127