Parr Instrument 6300 - Manual (Page 128)

G
B
OMB
R
INSE
C
ONTAINER
A
SSEMBLY
P a r r I n s t r u m e n t C o m p a n y 128
O
PERATION
(C
ONTINUED
)
Samples to be analyzed for chlorine should be spiked in
a manner to insure that the sample as-burned contains
less than 10% chlorine and liberates at least 5000 calo-
ries. Five thousand calories corresponds to roughly a
6.4 °C temperature rise in a 6300 Calorimeter.
Figure G-1
Vessel Rinse Container
1051DD
EXHAUST DIFFUSER
308VBAD MALE CONNECTOR
(1/4T-1/4NPTM)
HX0025TB062
1/4" TUBING X 4 FT LG
411VBAD REDUCER
(1/4T-3/8Tx)
221VBAD 3/8T NUT
222VBAD 3/8T FERRULE SET
1052DD
BOTTLE CAP
A138CA MALE CONNECTOR
(1/4T-1/8NPTM)
1.50
1053DD BOTTLE, 500ml
At the completion of the test, the collection bottle
should be unscrewed from the 1052DD Bottle Cap and
the contents of the combustion capsule added to the
collected washings. The bottle then may be capped and
labeled until the contents can be analyzed.
Most users find it useful to add the contents of the
rinsed combustion capsule to the washings collected in
the bottle.