beautypg.com

Program with suppression – Metrohm 754 Dialysis Unit User Manual

Page 27

background image

3 Operation

754 Dialysis Unit

24

3.3.2

Programming with the 732 IC Detector

Program without suppression

To dialyse in an IC system without suppression a program has to be

created for controlling the valves in the 733 IC Separation Center and

the 754 Dialysis Unit connected with cable 6.2143.200. The following

example program contains the necessary program steps.

PROGRAM
progr.type: cycle

number of cycles 1
0.0 valve A: fill

valve B: inject

remote: 1*******
2.0 valve B: fill
12.0 zero: on

valve B: inject
12.5 valve A: inject

remote 0*******
15.0 flag: end

Rinsing of sample loop

Rinsing of dialysis cell

Start of 754 Pump
Stop of acceptor solution
Trigger the auto-zero function

Transfer to sample loop
Injection (Õ Start evaluation)

Stop of 754 Pump
End of program

Program with suppression

To dialyze in an IC system with suppression a program has to be cre-

ated for controlling the valves in the 733 IC Separation Center and the

754 Dialysis Unit and 753 Suppressor Module connected with cable

6.2143.220. The following example program contains the necessary

program steps.

PROGRAM
progr.type: cycle

number of cycle 1
0.0 valve A: fill

valve B: inject

remote: *0*1****

2.0 valve B: fill
12.0 zero: on

valve B: inject

remote: *1******
12.5 valve A: inject

remote ***0****
15.0 flag: end

Rinsing of sample loop

Rinsing of dialysis cell

Resetting of the remote line for the

suppressor and start of 754 Pump
Stop of acceptor solution
Trigger the auto-zero function

Transfer to sample loop

Switch suppressor to next position
Injection (Õ Start evaluation)

Stop of 754 Pump
Program end

Programming

time

Transfer time

Dialysis time

Rinsing time

Programming

time

Rinsing time

Transfer time

Dialysis time