beautypg.com

Multiple crystal measurement channels, Electrode capacitance cancellation, Autolock – INFICON RQCM - Quartz Crystal Microbalance Research System User Manual

Page 16: Crystal face isolation, Fully intergated computer software, Inputs and outputs capability, Data acquisition, Multiple crystal measurement channels -2, Electrode capacitance cancellation -2, Autolock” -2

background image

RQCM – RESEARCH QUARTZ CRYSTAL MICROBALANCE

GENERAL DESCRIPTION

1-2

1.1.4

MULTIPLE CRYSTAL MEASUREMENT CHANNELS

The RQCM can be configured to measure up to three crystal measurement channels

simultaneously.

1.1.5

ELECTRODE CAPACITANCE CANCELLATION

The total quartz crystal impedance includes a shunt capacitance (due to the capacitance of

the crystal electrodes, cable and holder) in parallel with the series resonant arm. The total

current through the crystal is the sum of the current through the shunt capacitance plus

the current through the series resonant arm. The physical motion of the crystal is reflected

in the values of the L, R and C in the series arm of the crystal only, and therefore we want

to subtract out or otherwise cancel the current through the shunt electrode capacitance.

The Crystal Measurement Card includes a method of canceling the electrode capacitance

insuring that the measured crystal current does not include the current through the

electrode capacitance and therefore is essentially the current through the series resonant

arm of the crystal only.

1.1.6 “AUTOLOCK”

When the PLO loses lock, the VCO (Voltage Controlled Oscillator) is ramped up to the

maximum frequency at which time it is automatically reset to the minimum frequency

and a new scan is initiated.
To insure that the VCO ramps up in frequency, a small amount of quadrature current is

injected into the current to voltage buffer whenever the PLO is unlocked. This current is

equivalent to a shunt capacitance of about 1.5 pfd. As soon as lock is detected, the

quadrature current is turned off.

1.1.7

CRYSTAL FACE ISOLATION

The Crystal face is galvanically (transformer) isolated from earth ground. The Crystal

Face connection allows the crystal face electrode to be easily connected to an external

voltage or current source such as a potentiostat.

1.1.8

FULLY INTERGATED COMPUTER SOFTWARE

Computer software is included with each RQCM, allowing the user to set up, graph and

log frequency and resistance of the crystals from a computer. It also allows the setup,

graphing and logging of temperature and analog data – if the hardware is installed.

1.1.9

INPUTS AND OUTPUTS CAPABILITY

As an option, the RQCM can be outfitted with an I/O Card. This card provides eight

remote discrete inputs and eight relay outputs. These I/O’s can be used to monitor or

control external instruments and peripheral devices.

1.1.10 DATA

ACQUISITION

To support the simultaneous logging and display of additional analog information, such

as voltage, current, or temperature, the RQCM can be outfitted with an optional Data

Acquisition Card. This card supports three types of temperature sensors (RTD,

Thermocouple and Thermistor) as well as five scalable analog inputs.