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Teledyne GC-Pro/FID - Gas Chromatograph User Manual

Page 46

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Operation GC-Pro

FID

Teledyne

Analytical

Instruments

32

4.1 Equipment

The following supporting gases and hardware will be required to

operate the (standard) analyzer:

1. Fuel: A cylinder containing a hydrogen gas, zero gas quality

composition will be required to supply the fuel for the flame
ionization burner. The cylinder is to be equipped with an oil-free
metallic diaphragm regulator (dual stage).

2. Blanket Air: A cylinder of compressed air, zero gas quality will

be required to maintain the proper atmosphere within the cell.
The cylinder is to be equipped with an oil-free, dual stage,
metallic diaphragm regulator.

3. Carrier Gas: A cylinder of nitrogen gas, zero gas quality,

equipped with dual stage metallic diaphragm regulator is
required.

4. Span Gas: A cylinder or a permeation device system, capable of

generating known concentration of benzene and/or other
aromatic hydrocarbons of interest, will be required to standardize
the analyzer.

5. Sample Pressure Regulation: An oil-free, metallic diaphragm

regulator must be installed at the sample point when possible; see
Section 3.3.3 Gas Connections.

CAUTION: THE GASES USED MUST BE OF THE HIGHEST

QUALITY, ULTRA ZERO GRADES, AS SHOWN
BELOW. FAILURE TO DO SO WILL RESULT IN
CONTAMINATION AND FAILURE TO DETECT

AT

THE REQUIRED ACCURACY.

AIR: USE WATER PUMPED AIR WITH THC LESS
THAN 0.1 PPM. DO NOT USE OIL PUMPED AIR
UNDER ANY CIRCUMSTANCES.

FUEL: HYDROGEN GAS, 100%, ZERO QUALITY
WITH THC LESS THAN 0.5 PPM.

CARRIER GAS: NITROGEN GAS, ULTRA ZERO
GRADE WITH THC LESS THAN 0.05 PPM.