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Teledyne 2020 - Explosion proof thermal conductivity analyzer User Manual

Page 47

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Thermal Conductivity Analyzer

Operation 4

4-13

Teledyne Analytical Instruments

4.4.1 Zero Cal

The ZERO function in the MAIN MENU is used to enter the zero

calibration function. Zero calibration can be performed in either the auto-
matic or manual mode.

CAUTION: If you are zeroing the Cal Range by itself (multiple

application analyzers only), use

manual mode

zeroing.

If you want to calibrate ALL of the ranges at once
(multiple application analyzers only), use

auto mode

zeroing in the Cal Range.

Make sure the zero gas is flowing to the instrument. If you get a

CELL

CANNOT BE BALANCED message while zeroing skip to section 4.4.1.3.

4.4.1.1

Auto Mode Zeroing

Observe the precautions in sections 4.4 and 4.4.1, above.Scroll to

ZERO function buy using UP/DOWN control and enter the zero function
mode. The screen allows you to select whether the zero calibration is to be
performed automatically or manually. Use the UP/DOWN key to toggle
between

AUTO and MAN zero settling. Stop when AUTO appears, blinking,

on the display.

Select zero

mode: AUTO

Press

Enter

to begin zeroing.

####.## % H2 — N2

Slope=#.### C—Zero

The beginning zero level is shown in the upper left corner of the

display. As the zero reading settles, the screen displays and updates infor-
mation on

Slope= in ppm/second (unless the Slope starts within the accept-

able zero range and does not need to settle further). The system first does a
course zero, shown in the lower right corner of the screen as

C—Zero, for

approximate 3 min, and then does a fine zero, and displays

F—Zero, for

approximate 3 min.

Then, and whenever Slope is less than 0.01 for at least 3 min, instead

of Slope you will see a countdown:

9 Left, 8 Left, and so fourth. These are

software steps in the zeroing process that the system must complete, AF-