IKA C 5000 control Package 2/12 User Manual
Page 74

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IKA
-WERKE C 5000 control/duo-control Ver. 10 04.07
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Suspend carefully the decomposition vessel into the open measurement cell cover
until it reaches the stopper (1., see the following illustration).
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The decomposition vessel maintains a defined position in the holder on the fill head
by being lowered at the centre of the fill head by 0.8 mm (no. 2 in the following illus-
tration). A spring element then contacts the electrical ignition contact on the decom-
position vessel.
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The message "Bomb securely closed?" will appear. Ensure that the decomposition
vessel is properly closed and confirm with OK.
The message
%RPE
p
on the bottom line of the screen changes to a display of the
function key assignment
6WDUW
If the function key assignment
6WDUW
does not appear,
please check the ignition wire of the decomposition vessel. Take note of whether the
status is shown in a
6WDEOH
state on the display.
After each measurement, the measurement cell is adjusted so that normal starting
conditions are present for the next measurement. During this phase (about 3 to 5
minutes), “Unstable!!” is displayed in the process window of the measurement cell.
As long as this message is displayed, no measurements are possible in adiabatic or
isoperibolic operating modes. Experiments in dynamic mode can also be started
during the adjustment phase.
In addition to the adjustment requirements, the following conditions must be fulfilled
in order to start a measurement:
•
A measurement must be prepared
•
The maintenance function must not have been activated
•
The decomposition vessel must be removed and placed back in again
•
The ignition contact and the ignition wire of the decomposition vessel being
used must be in order.
Not until this point is the start button for the measurement cell enabled, i.e.,
6WDUW
appears on it.
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