IKA C 5000 control Package 2/12 - Manual (Page 67)

IKA  -WERKE C 5000 control/duo-control Ver. 10 04.07
3DJH
h
Open the decomposition vessel and check the crucible for any signs of incomplete
combustion. If combustion was not complete, the results of the experiment must not
be used for calibration. The experiment must be repeated.
i
Clean the decomposition vessel as described in Section 10.4 (or the Operating In-
structions for decomposition vessel C 5010/C 5012) and prepare the next experi-
ment.
j
Perform a number of calibration experiments for each decomposition vessel as de-
scribed in Section 9.1 “Charging the decomposition vessel with the calibration sub-
stance” and Section 9.2 “Calibration”, steps 1 - 7. For the number of calibrations
required, refer to standard in use. For example, DIN 51900 recommends at least
5 calibrations.
k
After the last calibration: activate 0HQX , open the &RQI menu window and then
open the %RPEV dialog box.
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cb
Using 7DE and 8S DUURZ 'RZQ DUURZ place the cursor on the number of the de-
composition vessel with which the calibration experiments have just been per-
formed.
For systems with WZR PHDVXUHPHQW FHOOV
Using 7DE and 8S DUURZ 'RZQ DUURZ place the cursor on the number of the
measurement cell and then on the decomposition vessel with which the calibration
experiments have just been performed.