Parr Instrument 6200 User Manual
Page 4
5
6200
Calorimeter Operating Instruction Manual
Appendix B – Calculations
B-1
Calculating the Heat of Combustion............................................................ B-1
General Calculations................................................................................... B-1
Thermochemical Corrections ...................................................................... B-2
ASTM and ISO Methods Differ.................................................................... B-3
Acid and Sulfur Corrections ........................................................................ B-4
ASTM Treatment for Acid and Sulfur .......................................................... B-6
ISO Calculations ......................................................................................... B-6
Spiking Samples ......................................................................................... B-7
Conversion to Other Moisture Bases .......................................................... B-7
Conversion to Net Heat of Combustion....................................................... B-7
Appendix C- Standardization
C-1
Standardizing the Calorimeter..................................................................... C-1
Standard Materials ...................................................................................... C-1
Automatic Statistical Calculations ............................................................... C-2
Appendix D - Communication Interfaces
D-1
Printer Port .................................................................................................. D-1
Balance Port................................................................................................ D-1
Mettler 011/012 Balance Interface .............................................................. D-1
Sartorius Balance Interface ......................................................................... D-2
Generic Interface......................................................................................... D-3
Run Date Template ..................................................................................... D-4
Ethernet Interface........................................................................................ D-5
Bar Code Port ............................................................................................. D-10
Network Data Devices................................................................................. D-10
Appendix E - Technical Service
E-1
Return for Repair......................................................................................... E-1
Appendix F – 6200 Calorimeter Parts & Diagrams
F-1
Principal Assemblies in Calorimeter............................................................ F-1
Parts List for A1279DD Controller Assembly .............................................. F-1
Parts List for Temperature Control Assembly ............................................. F-2
Parts List for A1284DD2 Stirrer Hub Assembly .......................................... F-2
Spare and Installation Parts List ................................................................. F-2
Parts List for Water Tank Assembly ............................................................ F-3
Parts List for Cooling Water Supply ............................................................ F-3
Parts List for Oxygen Filling System ........................................................... F-3
Parts List for 6200 Stirrer Motor and Drive.................................................. F-3
F-1
6200 Oxygen Bomb Calorimeter Cutaway Front ............................. F-4
F-2
6200 Oxygen Bomb Calorimeter Cutaway Rear.............................. F-5
F-3
A1279DD Control Schematic ........................................................... F-6
F-4
Oxygen Solenoid Assembly ............................................................. F-7
F-5 Water
Tank
Assembly......................................................................
F-8
F-6
A1311DD Circulating Pump Assembly ............................................ F-9
F-7
Temperature Control Assembly ....................................................... F-10
F-8
A1284DD2 Stirrer Hub Assembly .................................................... F-11
F-9
Stirrer Motor Assembly .................................................................... F-12
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