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LABEC M-MIA-A User Manual

Page 85

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Ultrasonic milk analyser

2.5. Electrolyte Replacement (for refillable electrode only).

The reference electrolyte needs to be refilled when the electrode has been
used for a long period, or when the internal electrolyte has dried up. To
accomplish this, follow the procedure described below.

- Remove the protective rubber cap or sleeve;
- Remove the protective rubber sleeve to expose the filling port of the

electrode;

- Remove the old reference electrolyte with a syringe;
- Fill the new reference electrolyte.

2.6. New electrolyte preparation:

- Open the KCl container;
- Add in de-ionized water until it reaches the level of 20 ml;
- Close the container and shake it to dissolve the KCl;
- Add in fresh electrolyte until it reaches the level of the refilling port. The

reference electrolyte used should be 3M(Mol) KCl;

- Replace the rubber sleeve.

2.7. Re-use the electrode.

- Rinse the liquid junction with de-ionized water.

If these steps fail to restore normal electrode response, you may attempt to
rejuvenate it (See: Electrode Rejuvenation).

2.8. Electrode cleaning

Electrodes which are mechanically intact can often be restored to normal
performance by one or combination of the following procedures.

- Salt deposits:
Dissolve the deposit by immersing the electrode in tap water for ten to fifteen
minutes. Then thoroughly rinse with de-ionized water. Wash the electrode pH
bulb in a little detergent and water. Rinse electrode tip in with de-ionized
water.

- Oil/Grease films:
Wash electrode pH bulb in a little detergent and water. Rinse electrode tip
with de-ionized water.

- Clogged Reference Junction:
pH electrodes have junction, which allows the internal fill solution of the
measuring electrode to leak out into the solution being measured. The

Operation manual

MRC.VER.01-02.10