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Hanna Instruments HI 83099 User Manual

Page 52

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103

102

OZONE

SPECIFICATIONS

Range

0.00 to 2.00 mg/L

Resolution

0.01 mg/L

Accuracy

±0.02 mg/L ±3% of reading at 25 °C

Typical EMC

±0.01 mg/L

Deviation
Light Source

Tungsten lamp with narrow band interference filter @ 525 nm

Method

Colorimetric DPD Method. The reaction between ozone and the DPD reagent causes a
pink tint in the sample.

REQUIRED REAGENTS

Code

Description

Quantity/test

HI 93757-0

DPD Powder Reagent

1 packet

HI 93703-52-0 Glycine Powder (Optional Reagent) 1 packet

REAGENT SETS

HI 93757-01

Reagents for 100 tests

HI 93757-03

Reagents for 300 tests

HI 93703-52

Glycine Powder, Optional Reagent for 100 tests

For other accessories see page 132.

IMPORTANT NOTE: Chlorine is a strong interferent for ozone determination. If the sample is suspected to
contain chlorine residues (free or total chlorine), please follow the

alternative measurement procedure

described below:
• Perform the Standard Measurement Procedure and take note of the reading:

value A.

• On a fresh sample perform the Additional Measurement Procedure and take note of the reading:

value B.

• Subtract reading

B from reading A to obtain the ozone concentration in mg/L:

mg/L (O

3

) =

value A – value B.

STANDARD MEASUREMENT PROCEDURE

• Select the

Ozone method using the procedure described

in the

Method Selection section (see page 12).

• Fill the cuvette with 10 mL of unreacted sample, up to

the mark, and replace the cap.

• Place the cuvette into the holder and close the lid.

Ozone

10 mL

• Select

Oxygen Demand, Chemical LR

(COD) method following one of the
procedures described in the

Method

Selection section (see page 12).

• Place the COD vial adapter in the

cuvet holder and ensure that the
adapter is well fit inside.

• Place the blank vial into the holder and push it completely down.

• Press the Zero key and the instrument will perform a zero sequence. If the zero sequence was

successfully done, the display will show “

-0.0-”. Now the meter is zeroed and ready for measurement.

• Remove the blank vial.

• Place the sample vial into the holder and push it completely down.

• Press

Read and the instrument will perform the reading.

• The instrument displays concentration in

mg/L of oxygen demand.

INTERFERENCES

Interference may be caused by:
Chloride (Cl¯) above 2000 mg/L.
Samples with higher chloride concentration should be diluted.

COD LR