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3 replacing parts of the msm‑hc – Metrohm 850 Professional IC Anion MSM-HC MCS Prep 1 User Manual

Page 112

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5.11 High Capacity Metrohm Suppressor Module (MSM-HC)

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102

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850 Professional IC – Anion MSM-HC – MCS – Prep 1

5.11.3.3

Replacing parts of the MSM-HC

It may be necessary to replace parts of the MSM-HC in the following
cases:

Loss of suppression capacity which cannot be eliminated (reduced
phosphate sensitivity and/or significant rise in the baseline).

Blockage of the MSM-HC which cannot be eliminated (solutions can
no longer be pumped through the suppressor).

Both the MSM-HC rotor A (49-3) and the MSM-HC connecting piece
(49-2) with its supply and discharge lines can be replaced.

Replacing parts of the MSM-HC

Replace parts of the MSM-HC as follows (see Figure 49, page 100):

1 Disconnecting the MSM-HC from the IC system

Switch off the instrument.

Disconnect the MSM-HC from the separation column, peristaltic
pump and detector.

2 Dismantling the MSM-HC

Unscrew union nut (49-1) from the MSM-HC housing (49-4).

Pull the MSM-HC connecting piece (49-2) and the MSM-HC rotor
A (49-3) out of the MSM-HC housing (49-4). The connecting
piece and the MSM-HC rotor A normally stick to one another – if
this is not the case: Take a sharp object, insert into the slot (49-5)
in the MSM-HC housing, and pull out the MSM-HC rotor A (49-3)
in this way.

Detach the MSM-HC connecting piece (49-2) from MSM-HC rotor
A (49-3).

3 Cleaning the new MSM-HC rotor A

Clean the sealing surface of the new MSM-rotor A (49-3) with
ethanol using a lint-free cloth.

4 Inserting the new MSM-HC rotor A

Caution

An incorrectly inserted MSM rotor A (49-3) can be destroyed
during start-up.