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Metrohm 850 Professional IC Anion MCS Prep 3 User Manual

Page 6

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Table of contents

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IV

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850 Professional IC –Anion – MCS – Prep 3

2.14 Sample preparation module (SPM) ................................... 40
2.14.1

General information on the SPM ............................................ 40

2.14.2

Connectors ............................................................................ 40

2.14.3

Inline sample preparation with the SPM ................................. 42

2.15 Peristaltic pump .................................................................. 46
2.15.1

Principle of the peristaltic pump ............................................. 46

2.15.2

Installing the peristaltic pump ................................................ 47

2.16 Injection valve ..................................................................... 51
2.16.1

Connecting the injection valve ............................................... 51

2.16.2

Mode of operation of the injection valve ............................... 52

2.16.3

Selecting the sample loop ...................................................... 53

2.17 Column thermostat ............................................................ 53

2.18 Metrohm Suppressor Module (MSM) ............................... 56
2.18.1

General information on the MSM .......................................... 56

2.18.2

Connecting the MSM ............................................................ 56

2.19 Metrohm CO

2

suppressor (MCS) ....................................... 59

2.19.1

General information on the MCS ........................................... 59

2.19.2

Connecting MCS ................................................................... 59

2.19.3

Installing the adsorption cartridges ........................................ 60

2.20 Conductivity detector ......................................................... 62

2.21 Connecting the instrument ................................................ 65
2.21.1

Connecting the instrument to the PC ..................................... 65

2.21.2

Connecting the instrument to mains supply ........................... 65

2.22 Guard column ..................................................................... 66

2.23 Separation column ............................................................. 68

3 Start-up

70

3.1

Initial start-up ..................................................................... 70

3.2

Conditioning ........................................................................ 71

4 Operation and maintenance

73

4.1

General information ........................................................... 73

4.1.1

Care ...................................................................................... 73

4.1.2

Maintenance by Metrohm Service .......................................... 73

4.1.3

Operation .............................................................................. 74

4.1.4

Shutting down ...................................................................... 74

4.2

Capillary connections ......................................................... 74

4.2.1

Operation .............................................................................. 74

4.3

Door ..................................................................................... 75

4.4

Eluent ................................................................................... 75

4.4.1

Production ............................................................................. 75

4.4.2

Operation .............................................................................. 76