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Figure 27, Neutralization and preconcentration, Figure 28 – Metrohm 850 Professional IC Anion MCS Prep 3 User Manual

Page 55: Injection and sequential suppression, Injection valve 1 (27-a) in position, Injection valve 2 (27-c), 2) onto the

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2 Installation

850 Professional IC –Anion – MCS – Prep 3

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45

The analyte ions are retained on the preconcentration column
(27-D) while the transfer solution flows to the waste container.

A

B

C

D

1

2

Figure 27

Neutralization and preconcentration

1

Sample

2

Transfer solution

A

Injection valve 1

B

SPM

C

Injection valve 2

D

Preconcentration column

3 Injection and sequential suppression

Injection valve 2 is switched:

– Injection valve 1 still is in position Inject.
Injection valve 2 (28-C) in position Inject.

With the eluent flow (28-3) the analyte ions retained on the pre-
concentration column (28-D) are rinsed onto the separation col-
umn (28-E).

The sequential suppression with the MSM (28-F) and the MCS fol-
lows after the separation.

C

F

D

E

3

Figure 28

Injection and sequential suppression

3

Eluent

C

Injection valve 2