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Brookfield CAP2000 Viscometer User Manual

Page 24

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Brookfield Engineering Labs., Inc.

Page 24

Manual No. M02-313-G0812

Note: A cone calibration should be performed when: 1) using a new cone for the first time,

2) switching between two cones of the same number and 3) verification of calibration

provides data outside of the acceptable range.

Refer to Tables III-5 and III-6 to choose the calibration fluid for the spindle being calibrated.

1. Turn on the CAP 2000+ Viscometer.

2. Attach solvent trap to coupling shaft.

3. Attach spindle.

4. Place appropriate amount of sample onto the center of the Viscometer plate directly below

the spindle.

5. Pull down the handle, locking it into the lowest position, placing the spindle in contact with

the plate.

6. Lower the solvent trap.

Note: The solvent trap must be utilized when calibrating to ensure proper temperature control.

7. Select the spindle to be calibrated by using the SPINDLE key.

8. Select YES for CALIBRATE and press ENTER.

9. Enter the appropriate values for temperature (°C) and viscosity (cP) value printed on the

label.

Note: Viscosity values are always entered in units of CENTIPOISE (cP) no matter what units

have been selected as unit of measure for normal operation.

100 cP = 1P; 1cP = 1mPa•s; 1000 cP = 1Pa•s

Note: The Viscometer temperature control must be identical to the specified temperature for

the viscosity standard when executing the calibration. Normally calibration will be at

25°C for “L” Series CAP Viscometers and 60°C for “H” Series CAP Viscometers.

10. Allow at least 30 minutes for thermal equilibrium of the plate, calibration fluid and spindle,

from instrument cold start.

11. Select the spindle speed.

All of the spindles used with the low torque CAP 2000+ instruments should be calibrated

at 100 RPM when using the recommended viscosity standard fluids. This practice will

calibrate the instrument at approximately the middle of the Full Scale Range.

Spindles used with the high torque CAP 2000+ and the recommended viscosity standard

fluids may be calibrated at any speed.

12. Press the RUN key to start the calibration.