Metrohm 896 Professional Detector – Amperometry - Manual (Page 5)

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Table of contents
2.896.0020 896 Professional Detector – Amperometry
￭￭￭￭￭￭￭￭ III
Table of contents
1 Introduction 1
1.1 Instrument description ......................................................... 1
1.2 Intended use ......................................................................... 2
1.3 Safety instructions ................................................................ 2
1.3.1 General notes on safety ........................................................... 2
1.3.2 Electrical safety ........................................................................ 2
1.3.3 Tubing and capillary connections ............................................. 3
1.3.4 Flammable solvents and chemicals ........................................... 4
1.3.5 Recycling and disposal ............................................................. 4
1.4 About the documentation ................................................... 4
1.4.1 Content and scope .................................................................. 4
1.4.2 Symbols and conventions ........................................................ 5
2 Overview of the instrument 6
2.1 Front ...................................................................................... 6
2.2 Rear ........................................................................................ 8
3 Installation 9
3.1 Setting up the instrument .................................................... 9
3.1.1 Packaging ................................................................................ 9
3.1.2 Checks .................................................................................... 9
3.1.3 Location .................................................................................. 9
3.1.4 Proposed setup ........................................................................ 9
3.2 Mounting base tray and bottle holder (optional) ............ 10
3.2.1 Removing / mounting the base tray ....................................... 10
3.2.2 Removing / mounting the bottle holder ................................. 12
3.3 Amperometric detector ...................................................... 15
3.4 Connecting the instrument ................................................ 15
3.4.1 Connecting the instrument to the PC ..................................... 15
3.4.2 Connecting the instrument to power supply .......................... 15
4 Start-up 17
4.1 Instrument test with dummy cell ...................................... 17
4.2 Testing the leak sensor ...................................................... 19
4.3 Testing the preheating capillary ....................................... 19
4.4 Testing the detector output capillary ............................... 20
4.5 Testing the measuring cell ................................................. 22
4.6 Deaerating the measuring cell .......................................... 24