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Metrohm 850 Professional IC Anion MCS Gradient User Manual

Page 7

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Table of contents

850 Professional IC –Anion – MCS – Gradient

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V

4.6

Inline filter ........................................................................... 82

4.6.1

Maintenance ......................................................................... 82

4.7

Inline sample preparation .................................................. 84

4.8

Rinsing the sample path .................................................... 84

4.9

Sample degasser ................................................................. 86

4.9.1

Operation .............................................................................. 86

4.10 Injection valve .................................................................... 86
4.10.1

Protection .............................................................................. 86

4.11 Metrohm Suppressor Module (MSM) ............................... 86
4.11.1

Protection .............................................................................. 86

4.11.2

Operation .............................................................................. 86

4.11.3

Maintenance ......................................................................... 87

4.12 Peristaltic pump .................................................................. 92
4.12.1

Operation .............................................................................. 92

4.12.2

Maintenance ......................................................................... 93

4.13 Metrohm CO

2

suppressor (MCS) ....................................... 95

4.13.1

Replacing the CO

2

adsorption cartridge ................................. 95

4.13.2

Regenerating the H

2

O adsorption cartridge ............................ 95

4.14 Conductivity detector ......................................................... 96
4.14.1

Maintenance ......................................................................... 96

4.15 Separation column ............................................................. 96
4.15.1

Separating efficiency .............................................................. 96

4.15.2

Protection .............................................................................. 97

4.15.3

Storage ................................................................................. 97

4.15.4

Regeneration ......................................................................... 97

4.16 Quality Management and validation with Metrohm ....... 98

5 Troubleshooting

99

5.1

Problems and their solutions ............................................. 99

6 Technical specifications

104

6.1

Reference conditions ........................................................ 104

6.2

Instrument ......................................................................... 104

6.3

Leak sensor ....................................................................... 104

6.4

Ambient conditions .......................................................... 104

6.5

Housing ............................................................................. 105

6.6

Eluent degasser ................................................................ 105

6.7

High pressure pump ......................................................... 105

6.8

Sample degasser ............................................................... 106

6.9

Injection valve ................................................................... 106