Hanna Instruments HI 83200C User Manual

Page 44

Nickel LR

• Press

Timer and the display will show a countdown prior to adding reagent C or, alternatively, wait

for 15 minutes. Add one packet of HI 93740C-0 EDTA reagent to each beaker, cap and swirl to mix
until completely dissolved.

• Fill one cuvette up to the mark with 10 mL of the blank.

• Place the cuvette into the holder and close the lid.

• Press the

Zero key. The display will show “-0.0-” when the meter is zeroed and ready for

measurement.

• Fill a second cuvette up to the mark with 10 mL of the reacted sample.

• Insert the second cuvette into the instrument.

• Press

Read to start the reading. The instrument displays the results in mg/L of nickel.

Note: a temperature above 30°C may cause turbidity. In this case, before zeroing and taking
readings, add 2-3 drops of Dispersing Agent (HI 93703-51) to each cuvette and swirl until turbidity
is removed.

Nickel LR

NICKEL LOW RANGE

SPECIFICATIONS

Range

0.000 to 1.000 mg/L

Resolution

0.001 mg/L

Accuracy

±0.010 mg/L ±7% of reading at 25 °C

Typical EMC

±0.001 mg/L

Deviation
Light Source

Tungsten lamp with narrow band interference filter @ 575 nm

Method

Adaptation of the PAN method. The reaction between nickel and the reagents causes
an orange tint in the sample.

REQUIRED REAGENTS

Code

Description

Quantity

HI 93740

A-0

Phthalate-phosphate

2 packets

HI 93740

B-0

0.3% PAN indicator

2 mL

HI 93740

C-0

EDTA

2 packets

HI 93703-51

Dispersing Agent

4-6 drops (only when necessary, see note)

REAGENT SETS

HI 93740-01 Reagents for 50 tests
HI 93740-03 Reagents for 150 tests
For other accessories see page 128.

MEASUREMENT PROCEDURE

• Select the

Nickel LR method using the procedure described in

the

Method Selection section (see page 12).

Note: for best results perform your tests between 20-24°C.

• Fill one graduated beaker with 25 mL of deionized water

(blank) and another one with 25 mL of sample.

• Add the content of one packet of HI 93740A-0 Phthalate-

phosphate reagent to each beaker. Cap and swirl gently until
the reagent is dissolved.
Note: If sample contains iron (Fe

), it is important that all

powder be dissolved completely before continuing with following
step.

• Add 1 mL of HI 93740B-0 0.3% PAN solution to each

beaker, cap and swirl to mix.

10 mL