beautypg.com

Metrohm 930 Compact IC Flex ChS/Deg User Manual

Page 96

background image

6.1

■■■■■■■■■■■■■■■■■■■■■■

88

■■■■■■■■

930 Compact IC Flex ChS/Deg (2.930.1260)

Problem

Cause

Remedy

Precision problems -
the measured values
are highly scattered.

Injection valve – Sample
loop.

Inspect the installation of the sample loop (see
"Optional: Exchanging the sample loop",
page 27)
.

Sample – There are gas
bubbles in the sample.

Use the sample degasser .

Sample – The rinsing vol-
ume is too small.

Increase the rinsing time (see Chapter 5.13,
page 81)
.

Injection valve – Defective.

Request Metrohm Service.

Vacuum is not being
built

Eluent degasser – Vacuum
connection on the rear of
the instrument is not
(tightly) sealed.

Seal the Vacuum connector tightly with a
threaded stopper (6.1446.040).