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Metrohm 930 Compact IC Flex Oven/SeS/PP/Deg User Manual

Page 6

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Table of contents

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IV

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930 Compact IC Flex Oven/SeS/PP/Deg (2.930.2560)

3.13 Peristaltic pump .................................................................. 35
3.13.1

Installing the peristaltic pump ................................................ 35

3.13.2

Mode of operation for the peristaltic pump ........................... 40

3.14 Metrohm CO

2

Suppressor (MCS) ....................................... 41

3.14.1

General information on MCS ................................................. 41

3.14.2

Connecting the MCS ............................................................. 42

3.14.3

Installing adsorption cartridges .............................................. 43

3.15 Installing the detector ........................................................ 45

3.16 Connecting the sample degasser (optional) ..................... 45

3.17 Connecting the instrument to a computer ....................... 47

3.18 Connecting the instrument to the power supply ............. 48

3.19 Initial start-up ..................................................................... 49

3.20 Connecting and rinsing the guard column ....................... 51

3.21 Connecting the separation column ................................... 53

3.22 Conditioning ........................................................................ 57

4 Operation

59

5 Operation and maintenance

60

5.1

IC system ............................................................................. 60

5.1.1

Operation .............................................................................. 60

5.1.2

Care ...................................................................................... 60

5.1.3

Maintenance by Metrohm Service .......................................... 60

5.1.4

Shutting down and starting back up ...................................... 61

5.2

Capillary connections ......................................................... 62

5.3

Servicing the door .............................................................. 62

5.4

Column oven – replacing the capillaries ........................... 62

5.5

Handling the eluent ............................................................ 64

5.5.1

Manufacturing eluent ............................................................ 64

5.5.2

Changing the eluent .............................................................. 65

5.6

Servicing the eluent degasser ........................................... 65

5.7

Notes on operating the high-pressure pump ................... 66

5.8

Servicing the high-pressure pump .................................... 67

5.9

Servicing the inline filter .................................................... 80

5.10 Servicing the pulsation absorber ...................................... 83

5.11 Injection valve ..................................................................... 83

5.12 Suppressor .......................................................................... 83
5.12.1

Notes for operating the suppressor ........................................ 83

5.12.2

Taking care of the suppressor housing ................................... 84

5.12.3

Servicing the suppressor ........................................................ 84