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Metrohm 850 Professional IC AnCat MCS User Manual

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Table of contents

850 Professional IC – AnCat – MCS

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III

Table of contents

1 Introduction

1

1.1

Instrument description ......................................................... 1

1.2

Intended use ......................................................................... 5

1.3

About the documentation ................................................... 5

1.3.1

Symbols and conventions ........................................................ 5

1.4

Safety instructions ................................................................ 6

1.4.1

General notes on safety ........................................................... 6

1.4.2

Electrical safety ........................................................................ 6

1.4.3

Tubing and capillary connections ............................................. 7

1.4.4

Flammable solvents and chemicals ........................................... 8

1.4.5

Recycling and disposal ............................................................. 8

2 Installation

9

2.1

About this chapter ................................................................ 9

2.2

Initial installation .................................................................. 9

2.3

Flow diagram ...................................................................... 11

2.4

Setting up the instrument .................................................. 14

2.4.1

Packaging .............................................................................. 14

2.4.2

Checks .................................................................................. 14

2.4.3

Location ................................................................................ 14

2.5

Capillary connections in the IC system ............................. 14

2.6

Rear of the instrument ....................................................... 16

2.6.1

Rollers and handle ................................................................. 16

2.6.2

Positioning and connecting the detector ................................ 19

2.6.3

Transport locking screws ....................................................... 21

2.6.4

Leak sensor ........................................................................... 21

2.6.5

Drainage tubing ..................................................................... 22

2.7

Capillary and cable feed-throughs .................................... 24

2.8

Eluent ................................................................................... 27

2.8.1

Connecting eluent bottle ....................................................... 27

2.9

Eluent degasser ................................................................. 31

2.10 High pressure pump ........................................................... 32
2.10.1

Capillary connections high pressure pump/purge valve ........... 32

2.10.2

Deaerating the high pressure pump ....................................... 35

2.11 Inline filter ........................................................................... 37

2.12 Pulsation damper ............................................................... 38

2.13 Sample degasser ................................................................. 40