beautypg.com

3 replacing parts of the msm – Metrohm 850 Professional IC AnCat MCS User Manual

Page 102

background image

4.11 Metrohm Suppressor Module (MSM)

■■■■■■■■■■■■■■■■■■■■■■

92

■■■■■■■■

850 Professional IC – AnCat – MCS

4.11.3.3

Replacing parts of the MSM

It may be necessary to replace parts of the MSM in the following cases:

Loss of suppression capacity which cannot be eliminated (reduced
phosphate sensitivity and/or significant rise in the baseline).

Blockage of the MSM which cannot be eliminated (solutions can no
longer be pumped through the suppressor).

Both the MSM rotor A (46-3) and the MSM connecting piece (46-2) with
its supply and discharge lines can be replaced.

Replacing parts of the MSM

Replace parts of the MSM as follows (see Figure 46, page 90):

1 Disconnecting the MSM from the IC system

Switch off the instrument.

Disconnect the MSM from the separation column, peristaltic
pump and detector.

2 Dismantling the MSM

Unscrew union nut (46-1) from the MSM housing (46-4).

Pull MSM connecting piece (46-2) and MSM rotor A (46-3) out of
the MSM housing (46-4). The MSM connecting piece and MSM
rotor A normally stick to one another - if this is not the case: Take
a sharp object, insert into the slot (46-5) in the MSM housing,
and pull out MSM rotor A (46-3) in this way.

Detach the MSM connecting piece (46-2) from MSM rotor A
(46-3).

3 Cleaning the new MSM rotor A

Clean the sealing surface of the new MSM rotor A (46-3) with
ethanol using a lint-free cloth.

4 Inserting the new MSM rotor A

Caution

An incorrectly inserted MSM rotor A (46-3) can be destroyed
during start-up.