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Turbidity calibration, 1 calibration standards, 2 indexing – Thermo Fisher Scientific TN100 Turbidimeter User Manual

Page 10: Calibration standards, Indexing

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Instruction Manual

TN-100/ T-100

5

2. Turbidity Calibration

Calibration Overview

The TN-100/T-100 turbidity meter was calibrated and tested prior to leaving the factory.

The meter kit now includes a set of prepared SDVB primary standards in plastic bottles

which are EPA-approved for meter calibration. This keeps the stock solutions for the

0.02, 20.0, 100 and 800 NTU standards ready to use and offers improved precision

and shelf life. A set of 4 empty vials for the standards are included in the meter kit.

Before using the meter for the first time, verify the meter calibration by reading back the

value for the prepared primary standard at the appropriate NTU value. This check is

recommended daily to check the meter prior to measuring a sample. When the

standard value drifts, retest with a vial of fresh standard solution. The 0.02 NTU

standard needs to read <0.1 NTU for acceptance.

A replacement set of the 4 standards in plastic bottles is available. These 60mL bottles

are identical to the bottles in the meter kit, so they can easily be carried in the case to

where the measurement needs to be taken. These standards are specifically made for

the TN-100/T-100 portable turbidity meters. The standards will not read to the stated

NTU value in other manufacturer’s turbidity meters.

2.1

Calibration Standards

We recommend that you use the following materials during calibration to achieve the

accuracy stated in this manual:

CAL 1: 800 NTU Calibration Standard

CAL 2: 100 NTU Calibration Standard

CAL 3: 20.0 NTU Calibration Standard

CAL 4: 0.02 NTU Calibration Standard

It is well known that diluted Formazin is unstable. If you choose to use Formazin to

calibrate the instrument, ensure that you are using a fresh stock suspension of

Formazin to achieve the accuracy quoted for the instrument. Calibration standards

offered are more stable than Formazin. For expiry date of calibration standard, please

refer to the expiration date indicated on the cap label.

It is important that the calibration standards are not violently shaken or agitated

because air entrapment in the fluid introduces an error factor during calibration

which subsequently will lead to an inaccurate measurement. Also, do not store in

freezing temperatures which causes irreversible shrinkage of the standards’

particles thus resulting to inaccurate calibration and measurement.

2.2

Indexing

Due to the high quality of the glass vials provided, indexing is not required. You only

need to align the mark on the vial with the mark on the meter. However, in order to

achieve a better accuracy of the measurement, you can proceed with indexing of the

vials. See Section 8.5 - Indexing a Vial on page 20 for more information.