Appendix b calibration check procedure, B.1 equipment, B.2 setup prrocedure – Brookfield R/S CPS Rheometer User Manual
Page 54
Brookfield Engineering Labs., Inc.
Page 54
Manual No. M08-218-B0212
• R/S-CPS+ Cone/Plate Rheometer with appropriate cables
• Temperature control apparatus
1
• Flat edged non-metal spatula
• Cone Spindle and Certified Mineral Oil Viscosity Standard:
One of the following
2
:
- RC3-25-1 Cone Spindle with Fluid B41000
- RC3-50-1 Cone Spindle with Fluid B11000
- RC3-50-2 Cone Spindle with Fluid B41000
- RC3-75-1 Cone Spindle with Fluid B4900
- RC3-75-2 Cone Spindle with Fluid B4900
• Rheo 3000 Applications Software loaded onto a PC (optional)
Reminders/Comments:
• A calibration check can be performed with or without software.
• The rheometer should always be allowed 10 minutes minimum to warm up.
• Never lift your rheometer by the head, shaft, coupling element, or measuring element
coupled to the machine.
• After the spindle has been lowered onto a sample, detach the spindle from the rheometer
head before raising the head.
• Total time to perform a calibration check is approximately 50 minutes.
1
Temperature Control apparatus consists of one of the following: Peltier System, Water bath, Oil Bath or Electronic Heat
2
Calibration check using either an RC3-25-1 or RC3-25-2 is not advised. To achieve the best results, use RC3-50-1.
•
Start Up
Rheometer
Load the
Viscosity
Standard
Zero
Rheometer
Set the Gap
Calibration
Check in
Stand-alone
Mode
Calibration
Check
Using
Rheo2000
Figure B-1: Flow Chart for Calibration Check Procedure
Appendix B Calibration Check Procedure
B.1 Equipment
B.2 Setup Prrocedure