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Teledyne 3000TA - General purpose trace oxygen analyzer User Manual

Page 45

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Trace Oxygen Analyzer

Operation 4

4-13

Teledyne Analytical Instruments

#### PPM Zero
4 Left=### ppm/s

The zeroing process will automatically conclude when the output is

within the acceptable range for a good zero. Then the analyzer automatically
returns to the

Analyze

mode.

4.4.1.2

Manual Mode Zeroing

Press

Zero

to enter the

Zero

function. The screen that appears allows

you to select between automatic or manual zero calibration. Use the

Δ∇ keys

to toggle between AUTO and MAN zero settling. Stop when MAN appears,
blinking, on the display.

Zero: Settling: Man
To Begin

Press

Enter

to begin the zero calibration. After a few seconds the first

of five zeroing screens appears. The number in the upper left hand corner is
the first-stage zero offset. The microprocessor samples the output at a prede-
termined rate. It calculates the differences between successive samplings and
displays the rate of change as Slope= a value in parts per million per second
(ppm/s).

#### ppm Zero
Slope=#### ppm/s

NOTE: It takes several seconds for the true

Slope

value to display. Wait about

10 seconds. Then, wait until

Slope

is sufficiently close to zero before

pressing Enter to finish zeroing .

Generally, you have a good zero when Slope is less than 0.05 ppm/s

for about 30 seconds. When Slope is close enough to zero, press

Enter

. In a

few seconds, the screen will update.

Once span settling completes, the information is stored in the

microprocessor, and the instrument automatically returns to the

Analyze

mode.

4.4.1.3

Cell Failure

Cell failure in the 3000TA is usually associated with inability to zero

the instrument down to a satisfactorily low ppm reading. When this occurs,
the 3000TA system alarm trips, and the LCD displays a failure message.

#.# ppm Anlz