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Appendix f - calibration check procedures – Brookfield DV1 Viscometer User Manual

Page 47

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Brookfield Engineering Laboratories, Inc.

Page 47

Manual No. M14-023

Appendix F - Calibration Check Procedures

For more help go to

www.brookfieldengineering.com and download the video.

Brookfield’s accuracy statement for viscometers used with standard spindles is +/-1% of Full Scale Range.

When measuring viscosity with a specific spindle rotating at a defined speed, the maximum viscosity that

can be measured is defined as Full Scale Range. For digital viscometers this value is easily determined by

pressing the “AUTORANGE” key. The display will show the Full Scale Range viscosity in cP or mPas

and the torque value will show 100%. Multiply the Full Scale Range viscosity by 1% to determine the

accuracy of any future measurement made with that spindle/speed combination.

When using the following accessory devices with your viscometer, the accuracy is +/-2%. Dimensional

tolerances in the accessory device allow for increase from +/-1% to +/-2%.

• Small Sample Adapter

• Thermosel

• UL Adapter

• DIN Adapter

• Spiral Adapter

The accuracy of the DV1 is verified using viscosity standard fluids, which are available from Brookfield

Engineering Laboratories or your local Brookfield agent. Viscosity standards are Newtonian, and there-

fore, have the same viscosity regardless of spindle speed (or shear rate). Viscosity standards, calibrated

at 25°C, are shown in Table F-1 (Silicone Oils) and Table F-2 (Mineral Oils).

Container size: For Viscosity Standards < 30,000 cP, use a 600 mL Low Form Griffin Beaker

having a working volume of 500 mL.
Inside Diameter: 3.25”(8.25cm)

Height: 4.75”(12.1cm)
For Viscosity Standards

30,000 cP, use the fluid container.

Note: Container may be larger, but may not be smaller.

Temperature:

As stated on the fluid standard label: (

+

/-) 0.1

°

C

Conditions:

The DV1 should be set according to the operating instructions. The water

bath must be stabilized at test temperature. Viscometers with the letters “LV

or “RV” in the model designation must have the guard leg attached, see Ap-

pendix G for more information on the guard leg).

Normal 25ºC Standard Fluids

Viscosity (cP)

Viscosity (cP)

High Temperature Standard Fluids

Three Viscosity/Temperatures**

5

5,000

HT-30,000

10

12,500

HT-60,000

50

30,000

HT-100,000

100

60,000

500

100,000

**25ºC, 93.3ºC, 149ºC

1,000

Refer to Brookfield catalog for more information

Table F-1